I have not succeeded yet in getting the stainless steel barrel to extrude easily, so I had a go at improving my aluminium extruder to remove the need for a fan.
A lot of heat is lost from the large flange on the top of the heater barrel and transfers by convection to the heatsink above and by conduction through the bolts.
When I stripped it down I noticed the bolts had loosened.
The PTFE had shrunk lengthways and expanded in diameter and was no longer making a good compression seal.
Although no plastic had escaped it had leaked under the PTFE.
I think it was leaking so slowly that it oxidized where it met the air and went hard, stopping further flow. I hadn't run it very long so it may have escaped eventually.
So PTFE is obviously no good in compression at these temperatures. I replaced it with PEEK, which is a shame because it is about ten times more expensive.
I also replaced the aluminium flange with an M8 x 25mm steel washer insulated from the barrel by a PEEK collar.
Here are the parts, the PEEK section is drilled in situ to get perfect alignment: -
And here it is assembled: -
I put some PTFE plumbing tape over the hot end of the PEEK before pushing it into the aluminium in an attempt to improve the seal.
The heatsink now runs at 80°C without the fan. I would have liked it to be lower but as long as it is below the glass transition of the filament and the clamp it should be OK. I tried insulating the bolts with PEEK washers but that only dropped the temperature by 5°C, so not really worth the effort.
After one heat cycle I noticed the bolts were not as tight as they should be so it looks like PEEK creeps a bit as well. Perhaps glass filled would be better.
It is disappointingly complex with lots of machined parts but it does work very well. The heater power has dropped to 50% from about 80-90% with the fan. ABS filament extrudes manually very easily and even HDPE only requires moderate force. I think actually having the long heatsink preheating the filament to just below the glass transition is probably a benefit.
It is too early to say whether this design will be reliable but other than the PEEK section leaking there isn't anything likely to fail. I don't mind making things that are difficult to make provided I only have to do it once.
I also have a much simpler design in mind that should achieve the same short transition zone.
Sunday, 11 January 2009
Thermal gradients
Although my last extruder design seems to work, I am not very happy with it. I don't like the little fan because it is noisy, it isn't easy to make and it is not very thermally efficient. The main heat loss is via the stainless steel bolts and from the big flange. The only reason those parts are needed is because the PTFE insulator does not have the necessary mechanical strength and stability.
Some time ago I tried to use stainless steel as the insulator because it is strong, self supporting and withstands high temperatures. That attempt failed because my thermal gradient was too long; the hot to cold transition was about 50mm. The extruder would run for a while but would always jam before an object was completed. Once the stainless steel barrel was fully up to temperature the amount of filament that is soft but not fluid is sufficient to provide too much resistance to be pushed. This theory was confirmed when I tried a soldering iron heater, which also has a long thermal gradient along its length.
I also tried PEEK as the metalab guys had success with it but that seemed to suffer from the same problem.
I had always intended to revisit the stainless steel idea with a shorter transition zone but when I saw Larry Pfeffer's stainless steel extruder it provided an extra idea of thinning down the pipe at the transition. That allows a short transition without too much heat loss or loss of mechanical strength.
I did some experimentation with this test set-up.
I made a heater with an integral aluminium barrel by turning some aluminium bar in my four jaw chuck, the first time I have used it. I used two 12Ω resistors in parallel this time instead of one 6.8Ω. They give a bit more power and possibly lower internal temperature inside the resistors.
I measured the temperature along the tube at 5mm intervals. The thermocouple is slightly smaller than the internal diameter of the tube. The weight of its cable causes the tip to rest on the roof of the tube and the other end rests on the floor of the filament exit. The thermocouple is itself encased in stainless steel, so there will be some heat leaked along it. Hopefully its casing is thin enough to have little effect compared to the much thicker tube it is sampling.
The heater was powered from a bench power supply and the voltage adjusted manually to give around 240°C in the middle of the heater block. That needed 9.4V which is 14W. I can feel substantial heat rising from it so some insulation would make it a lot more efficient. I have got some ceramic fibre kiln insulation for that, another tip I picked up from Larry's blog.
The first test was with a threaded tube with no constriction. The gradient is not far from linear, it falls off faster when hotter due to more convection and radiation from the hot section. If we assume ABS would be soft but very viscous between say 75°C and 125°C we see that it covers 45 to 60 i.e. 15mm.
I then turned a 10mm section of the tube down from 6.4mm to 4.5mm. The internal diameter of the tube is about 3.6mm so that gives a wall thickness of 0.45mm. That made the gradient steeper between 35mm and 40mm but the length of the perceived problem zone gets bigger. I am not sure how Larry gets away without a heatsink. I think he is using thicker pipe so there is a much bigger difference between the conduction of the constricted section and the rest. Also it takes a long time for the problem to become apparent because heat travels slowly down the pipe.
The final test was done with a heatsink attached just above the constriction. The centre of the heatsink only reached about 28°C. The aluminium block I used to connect it got hotter but was still comfortable to touch so less than 50°C.
The gradient between 30mm and 40mm is now much steeper. Odd that it is not between 25mm and 35mm where the constriction is. Almost like there is a 5mm offset in the readings. Anyway the 125°C to 75°C transition is now only about 3mm.
If we assume the temperature difference across the constriction is 210°C - 80°C = 130°C, the conducted heat loss is temperature difference × thermal conductivity × cross sectional area / length. So 130 × 17 × π × ((2.25×10-3)2 - (1.8×10-3)2) / 10×10-3 = ~1.3W, about 1/3 of the loss through the bolts and PTFE in my previous design.
So it looks promising, I need to add a nozzle and some insulation and see if it will extrude.
Some time ago I tried to use stainless steel as the insulator because it is strong, self supporting and withstands high temperatures. That attempt failed because my thermal gradient was too long; the hot to cold transition was about 50mm. The extruder would run for a while but would always jam before an object was completed. Once the stainless steel barrel was fully up to temperature the amount of filament that is soft but not fluid is sufficient to provide too much resistance to be pushed. This theory was confirmed when I tried a soldering iron heater, which also has a long thermal gradient along its length.
I also tried PEEK as the metalab guys had success with it but that seemed to suffer from the same problem.
I had always intended to revisit the stainless steel idea with a shorter transition zone but when I saw Larry Pfeffer's stainless steel extruder it provided an extra idea of thinning down the pipe at the transition. That allows a short transition without too much heat loss or loss of mechanical strength.
I did some experimentation with this test set-up.
I made a heater with an integral aluminium barrel by turning some aluminium bar in my four jaw chuck, the first time I have used it. I used two 12Ω resistors in parallel this time instead of one 6.8Ω. They give a bit more power and possibly lower internal temperature inside the resistors.
I measured the temperature along the tube at 5mm intervals. The thermocouple is slightly smaller than the internal diameter of the tube. The weight of its cable causes the tip to rest on the roof of the tube and the other end rests on the floor of the filament exit. The thermocouple is itself encased in stainless steel, so there will be some heat leaked along it. Hopefully its casing is thin enough to have little effect compared to the much thicker tube it is sampling.
The heater was powered from a bench power supply and the voltage adjusted manually to give around 240°C in the middle of the heater block. That needed 9.4V which is 14W. I can feel substantial heat rising from it so some insulation would make it a lot more efficient. I have got some ceramic fibre kiln insulation for that, another tip I picked up from Larry's blog.
The first test was with a threaded tube with no constriction. The gradient is not far from linear, it falls off faster when hotter due to more convection and radiation from the hot section. If we assume ABS would be soft but very viscous between say 75°C and 125°C we see that it covers 45 to 60 i.e. 15mm.
I then turned a 10mm section of the tube down from 6.4mm to 4.5mm. The internal diameter of the tube is about 3.6mm so that gives a wall thickness of 0.45mm. That made the gradient steeper between 35mm and 40mm but the length of the perceived problem zone gets bigger. I am not sure how Larry gets away without a heatsink. I think he is using thicker pipe so there is a much bigger difference between the conduction of the constricted section and the rest. Also it takes a long time for the problem to become apparent because heat travels slowly down the pipe.
The final test was done with a heatsink attached just above the constriction. The centre of the heatsink only reached about 28°C. The aluminium block I used to connect it got hotter but was still comfortable to touch so less than 50°C.
The gradient between 30mm and 40mm is now much steeper. Odd that it is not between 25mm and 35mm where the constriction is. Almost like there is a 5mm offset in the readings. Anyway the 125°C to 75°C transition is now only about 3mm.
If we assume the temperature difference across the constriction is 210°C - 80°C = 130°C, the conducted heat loss is temperature difference × thermal conductivity × cross sectional area / length. So 130 × 17 × π × ((2.25×10-3)2 - (1.8×10-3)2) / 10×10-3 = ~1.3W, about 1/3 of the loss through the bolts and PTFE in my previous design.
So it looks promising, I need to add a nozzle and some insulation and see if it will extrude.
Friday, 9 January 2009
Heater in a hurry hack
The heater in my last design has two layers of Cerastil that take 24 hours each to cure and the bobbin takes some time to machine. Attaching the wires and winding the coil is quite fiddly. Looking for a short cut I wondered if we could use power resistors. I had this one lying around to play with.
Unfortunately it is only rated for operation up to 200°C. In fact the datasheet says "It is essential that the maximum hot spot temperature of 220°C is not exceeded". Curious to see why, I put enough voltage across it to heat it up to 240°C. That turned out to be about 75W. It seemed quite happy at that temperature for several hours.
It is too big really for an extruder so I bought some smaller 10 Watt ones for £1.42 each.
These are only rated for 165°C but what the heck. I heated a 6.8Ω one to 300°C. At about 180°C it produces a little smoke but that soon goes. At 280°C it starts to smell bad, but at 240°C it seems happy. I left one powered up for a few days. The writing disappears and the connection tags oxidise, but its resistance is stable.
To make a heater I cut a 19mm x 19mm x 8mm block of aluminium from a bar, drilled a 5mm hole through it and tapped it to M6 to fit a heater barrel. The mounting holes of the resistor are big enough for M2.5 but there is not enough room for the head, or a nut. M2 is a bit weedy so instead I used 8BA bolts. These need a 2.8mm hole for tapping. A simpler solution would be to just file a flat on the head of an M2.5 bolt, drill a clearance hole and use a nut on the other side.
Here is the full assembly: -
I put heatsink compound on the M6 thread and under the resistor. I attached tinned copper wires with 300°C solder and insulated them with PTFE sleeving.
I have run the assembly for a couple of days and it held up. I am loath to recommend something which is unsound engineering, but it does seem a simple and robust solution as long it lasts a reasonable amount of time, say 1000 hours. Replacement is easy because the most time consuming thing is making the block which is reusable. I expect there might be some matching crimp connections to avoid the high temperature solder.
Quite a lot of heat is lost from the large surface area so some insulation would be a good idea.
Unfortunately it is only rated for operation up to 200°C. In fact the datasheet says "It is essential that the maximum hot spot temperature of 220°C is not exceeded". Curious to see why, I put enough voltage across it to heat it up to 240°C. That turned out to be about 75W. It seemed quite happy at that temperature for several hours.
It is too big really for an extruder so I bought some smaller 10 Watt ones for £1.42 each.
These are only rated for 165°C but what the heck. I heated a 6.8Ω one to 300°C. At about 180°C it produces a little smoke but that soon goes. At 280°C it starts to smell bad, but at 240°C it seems happy. I left one powered up for a few days. The writing disappears and the connection tags oxidise, but its resistance is stable.
To make a heater I cut a 19mm x 19mm x 8mm block of aluminium from a bar, drilled a 5mm hole through it and tapped it to M6 to fit a heater barrel. The mounting holes of the resistor are big enough for M2.5 but there is not enough room for the head, or a nut. M2 is a bit weedy so instead I used 8BA bolts. These need a 2.8mm hole for tapping. A simpler solution would be to just file a flat on the head of an M2.5 bolt, drill a clearance hole and use a nut on the other side.
Here is the full assembly: -
I put heatsink compound on the M6 thread and under the resistor. I attached tinned copper wires with 300°C solder and insulated them with PTFE sleeving.
I have run the assembly for a couple of days and it held up. I am loath to recommend something which is unsound engineering, but it does seem a simple and robust solution as long it lasts a reasonable amount of time, say 1000 hours. Replacement is easy because the most time consuming thing is making the block which is reusable. I expect there might be some matching crimp connections to avoid the high temperature solder.
Quite a lot of heat is lost from the large surface area so some insulation would be a good idea.
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